HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dimethoxyaniline → HCID 22732517, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dimethoxyaniline | HCID 66301 | — |
| Reactant | 4-Chloro-6-methyl-2-(pyridin-2-yl)pyrimidine | HCID 2763395 | — |
| Product | HCID 22732517 | HCID 22732517 | — |
Reaction Steps
The title compound was prepared from a mixture of 4-chloro-6-methyl-2-(2-pyridinyl)pyrimidine (50 mg, 0.243 mmol) and 3,5-dimethoxyaniline (56 mg, 0.365 mmol) similar to Example 92 and isolated as a tan solid (21 mg, 26%). 1H NMR (CDCl3): 8.83–8.81 (m, 1H), 8.49–8.46 (m, 1H), 7.86–7.80 (m, 1H), 7.39–7.35 (m, 1H), 6.99 (s, 1H), 6.70 (s, 1H), 6.53 (d, J=2.4 Hz, 2H), 6.30 (t, J=2.3 Hz, 1H), 3.82 (s, 6H), 2.51 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07226927B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-2776d27c815848e7b6cd77ed422bd8ac |
| Source note | uspto-grants-2007_06 |