HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Chloro-m-anisidine → HCID 22732388, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Chloro-m-anisidine | HCID 75460 | — |
| Reactant | HCID 22732394 | HCID 22732394 | — |
| Product | HCID 22732388 | HCID 22732388 | — |
Reaction Steps
The title compound was prepared from 4-chloro-2-(2,6-dichloro-4-pyridinyl)-6-trifluoromethyl-pyrimidine (52 mg, 0.159 mmol) and 2-chloro-5-methoxyaniline (40 mg, 0.255 mmol) similar to Example 160 and was isolated as a yellow crystalline solid (13 mg, 0.029 mmol, 18%). 1H NMR (CDCl3): 8.27 (s, 2H), 7.76 (s, br, 1H), 7.40 (s, 1H), 7.38 (s, 1H), 7.02 (s, 1H), 6.77 (m, 1H), 3.90 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07226927B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-5645308f54a948f4b1e2e25c6b4f2919 |
| Source note | uspto-grants-2007_06 |