HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-4-methoxybenzoic acid → HCID 22732396, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-4-methoxybenzoic acid | HCID 17823 | — |
| Reactant | 4-Chloro-2-(2-pyrazinyl)-6-(trifluoromethyl)pyrimidine | HCID 22732367 | — |
| Product | HCID 22732396 | HCID 22732396 | — |
Reaction Steps
The title compound was prepared from 4-chloro-2-(2-pyrazinyl)-6-trifluoromethylpyrimidine (40 mg, 0.154 mmol) and 5-carboxy-2-methoxyaniline (38 mg, 0.231 mmol), similar to Example 180 and was isolated as an off white solid (20 mg, 33%). 1H NMR (CDCl3): 9.99 (brs, 1H), 9.660 (d, J=1.5 Hz, 1H), 8.86 (m, 3H), 7.80 (d, 2H), 7.2 (m, 2H), 3.94 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07226927B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-2ba0342c03cb4a069f692c5ece0a5b9f |
| Source note | uspto-grants-2007_06 |