HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-5-chlorobenzophenone → N-(2-benzoyl-4-chloro-phenyl)-2-fluoro-benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-5-chlorobenzophenone | HCID 12870 | — |
| Reactant | 2-Fluorobenzenesulphonyl chloride | HCID 137761 | — |
| Product | N-(2-benzoyl-4-chloro-phenyl)-2-fluoro-benzenesulfonamide | HCID 11315279 | — |
Reaction Steps
The title compound was prepared according to the general procedure for the synthesis of N-Aryl-benzenesulfonamides previously described using (2-amino-5-chloro-phenyl)-phenyl-methanone and 2-fluoro-benzenesulfonyl chloride. 1H NMR (CDCl3): δ (ppm): 6.88–6.93 (m, 1H), 7.16–7.20 (m, 1H), 7.38 (d, J=6.4 Hz, 1H), 7.41–7.46 (m, 4H), 7.52 (m, 2H), 7.58–7.62 (m, 1H), 7.70 (d, J=8.8 Hz, 1H), 7.81–7.85 (m, 1H), 10.10 (s, 1H). MS: m/z 390.0 (M++1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07227035B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-9a3a4ba2cd33423597352c3ca25084df |
| Source note | uspto-grants-2007_06 |