HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-5-chlorobenzophenone → N-(2-benzoyl-4-chloro-phenyl)-3-fluoro-benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-5-chlorobenzophenone | HCID 12870 | — |
| Reactant | 3-Fluorobenzenesulfonyl Chloride | HCID 2734258 | — |
| Product | N-(2-benzoyl-4-chloro-phenyl)-3-fluoro-benzenesulfonamide | HCID 11372710 | — |
Reaction Steps
The title compound was prepared according to the general procedure for the synthesis of N-Aryl-benzenesulfonamides previously described using (2-amino-5-chloro-phenyl)-phenyl-methanone and 3-fluoro-benzenesulfonyl chloride. 1H NMR (CDCl3): δ (ppm): 7.00–7.05 (m, 1H), 7.35 (m, 1H), 7.37 (m, 1H), 7.39–7.44 (m, 4H), 7.37–7.43 (m, 4H), 7.45–7.46 (m, 1H), 7.49–7.50 (m, 1H), 7.51–7.52 (m, 2H), 7.58–7.62 (m, 1H), 9.80 (s, 1H). MS: m/z 390.0 (M++1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07227035B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-b27d7a41987c424f87511cae2525f09b |
| Source note | uspto-grants-2007_06 |