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HRID1766226

反应详情

EQUATION

反应方程式

HRID 1766226 的结构方程式

REACTANTS

反应物

2
结构：Cl.c1ccncc1
HCID10176127

Pyridine hydrochloride

C5H6ClN

结构：COc1cc(C)c2c(c1)c(C1CCN(C)CC1)cn2Cc1ccccc1
HCID69431313

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(O)cc2c(C3CCN(C)CC3)cn(Cc3ccccc3)c12
HCID69432444

未命名化合物

收率 60.2%

PROCEDURE

实验过程

By a method similar to Preparation 8, using 1-benzyl-5-methoxy-7-methyl-3-(1-methylpiperdin-4-yl)-1H-indole (1.62 g) and pyridine hydrochloride (25 g) to afford 0.936 g (60%) of the title compound: Mass spectrum (ion spray): m/z=335 (M+1).

WORKUP

后处理

  1. customBy a method similar to Preparation 8