HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 21110332, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Aminobenzophenone | HCID 14346 | — |
| Reactant | 4-Propylbenzoyl chloride | HCID 104293 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21110332 | HCID 21110332 | 78.4% |
Reaction Steps
Reaction of 4-aminobenzophenone (99 mg, 0.51 mmol) in THF (6 mL) with 4-propylbenzoyl chloride (100 μL, 0.65 mmol) in presence of triethylamine (90 μL, 0.65 mmol) according to method A gave N-(4-benzoyl-phenyl)-4-propyl-benzamide (136 mg, 0.40 mmol, 78% yield) as a white powder after purification by chromatography on silica gel (eluent EtOAc/DCM 0/100 to 5/95).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07230020B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-7766f806056d4d4fb91c412bffc5514a |
| Source note | uspto-grants-2007_06 |