HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Anisoyl chloride → HCID 832645, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Anisoyl chloride | HCID 7477 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Aminobenzophenone | HCID 14346 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 832645 | HCID 832645 | 98% |
Reaction Steps
Reaction of 4-aminobenzophenone (98 mg, 0.51 mmol) in THF (6 mL) with p-anisoyl chloride (90 μL, 0.65 mmol) in presence of triethylamine (90 μL, 0.65 mmol) according to method A gave N-(4-benzoyl-phenyl)-4-methoxy-benzamide (165 mg, 0.50 mmol, 98% yield) as a white powder after purification by washing the crude product with ethyl acetate and hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07230020B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-9cb1fb4d3af9430c90934d965313b73e |
| Source note | uspto-grants-2007_06 |