HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 21110277, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Propylbenzoyl chloride | HCID 104293 | — |
| Reactant | 4-Chloro-2-methylbenzo[d]thiazol-5-amine | HCID 11217857 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21110277 | HCID 21110277 | 52% |
Reaction Steps
Reaction of 4-chloro-2-methyl-benzothiazol-5-ylamine (50 mg, 0.25 mmol) in THF (1.5 mL) with 4-propylbenzoyl chloride (90 μL, 0.56 mmol) in presence of triethylamine (0.5 mL) according to method A gave N-(4-Chloro-2-methyl-benzothiazol-5-yl)-4-propyl-benzamide (44 mg, 0.13 mmol, 52% yield) as a orange powder after crystallisation in hexane and methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07230020B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-e300f24df87b4dc48ab141761c8f9d5e |
| Source note | uspto-grants-2007_06 |