Acetic Acid → HCID 69352356, compound

HRID 1766363Notes

Reaction equation

HRID 1766363 reaction equation
[CH3:1]/[C:2](/[NH2:6])=[CH:3]\[C:4]#[N:5].[CH3:7][C:8]1[CH:9]=[C:10]([CH:12]=[CH:13][CH:14]=1)N.C(O)(=O)C>O>[CH3:7][C:8]1[CH:14]=[C:13]([NH:6][C:2]([CH3:1])=[CH:3][C:4]#[N:5])[CH:12]=[CH:10][CH:9]=1

Participants

5

Reactant 3

HCID 176Acetic AcidHCID 7934m-ToluidineHCID 53247203-Aminocrotonitrile

Product 1

HCID 69352356HCID 69352356, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

3-Aminocrotonitrile (5.0 g, 60.9 mmol), 3-methylaniline (7.18 g, 66.99 mmol) and acetic acid (6.22 g, 103.5 mmol) are dissolved in water (20 ml). The reaction mixture is stirred at room temperature for 60 minutes and the precipitate is isolated.

Workup

  1. customthe precipitate is isolated

Sources & evidence

ORD record
ord-480122e5c4884dafb7230a7c6039e4e2
Source dataset
uspto-grants-2007_06
Patent number
US07230017B2

Reaction notes

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