Acetic Acid → HCID 69353307, compound

HRID 1766364Notes

Reaction equation

HRID 1766364 reaction equation
[CH3:1]/[C:2](/[NH2:6])=[CH:3]\[C:4]#[N:5].[Cl:7][C:8]1[CH:9]=[C:10]([CH:12]=[CH:13][CH:14]=1)N.C(O)(=O)C>O>[Cl:7][C:8]1[CH:14]=[C:13]([NH:6][C:2]([CH3:1])=[CH:3][C:4]#[N:5])[CH:12]=[CH:10][CH:9]=1

Participants

5

Reactant 3

HCID 176Acetic AcidHCID 79323-ChloroanilineHCID 53247203-Aminocrotonitrile

Product 1

HCID 69353307HCID 69353307, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

3-Aminocrotonitrile (5.0 g, 60.9 mmol), 3-chloroaniline (8.55 g, 66.99 mmol) and acetic acid (6.22 g, 103.5 mmol) are dissolved in water (20 ml). The reaction mixture is stirred at room temperature for 60 minutes and the precipitate is isolated.

Workup

  1. customthe precipitate is isolated

Sources & evidence

ORD record
ord-f9bc4cb362cc48c1aa615728366935a2
Source dataset
uspto-grants-2007_06
Patent number
US07230017B2

Reaction notes

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