HCID 18604804, compound → HCID 178462255, compound

HRID 1766637Notes

Reaction equation

HRID 1766637 reaction equation
[NH2:1][C@:2]1([C@H:10]([CH3:12])[OH:11])[O:7][C:5](=[O:6])[C:4]([OH:8])=[C:3]1[O-:9].[NH2:13][C@H:14]([C:20](Cl)=[O:21])[CH2:15][CH2:16][CH2:17][CH2:18][NH2:19]>N1C=CC=CC=1>[NH2:13][C@H:14]([C:20]([OH:21])=[O:6])[CH2:15][CH2:16][CH2:17][CH2:18][NH2:19].[NH2:1][C@:2]1([C@H:10]([CH3:12])[OH:11])[O:7][C:5](=[O:6])[C:4]([OH:8])=[C:3]1[O-:9]

Participants

4

Reactant 2

HCID 18604804HCID 18604804, compoundHCID 178462254HCID 178462254, compound

Product 1

HCID 178462255HCID 178462255, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

6-Deoxyamino ascorbate (5 mmoles) is reacted with lysyl chloride (7 mmoles) in dry pyridine and the reaction product is worked up according to Cousine et al. It is crystallized from ethanol.

Workup

  1. customis crystallized from ethanol

Sources & evidence

ORD record
ord-45ba94b562f6402497bf6b7268de3f3f
Source dataset
uspto-grants-2007_06
Patent number
US07230124B2

Reaction notes

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