HCID 12378858, compound → HCID 178462256, compound

HRID 1766638Notes

Reaction equation

HRID 1766638 reaction equation
[NH2:1][C@:2]1([C@H:10]([CH3:12])[OH:11])[O:7][C:5](=[O:6])[C:4]([OH:8])=[C:3]1[O-:9].[NH:13]1CCC[C@H]1C(Cl)=O>N1C=CC=CC=1>[NH:13]1[CH2:10][CH2:2][CH2:3][C@H:4]1[C:5]([OH:7])=[O:6].[NH2:1][C@:2]1([C@H:10]([CH3:12])[OH:11])[O:7][C:5](=[O:6])[C:4]([OH:8])=[C:3]1[O-:9]

Participants

4

Reactant 2

HCID 12378858HCID 12378858, compoundHCID 178462254HCID 178462254, compound

Product 1

HCID 178462256HCID 178462256, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

6-Deoxyamino ascorbate (5 mmoles) is reacted with prolyl chloride (7 mmoles) in dry pyridine and worked up by the method as described above and crystallized from ethanol.

Workup

  1. customcrystallized from ethanol

Sources & evidence

ORD record
ord-1e1f36dd71e64d359103d054f55389f4
Source dataset
uspto-grants-2007_06
Patent number
US07230124B2

Reaction notes

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