Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1766685Generated: November 1, 2026

Diethyl Oxalate → HCID 21110635, compound

https://huagongshe.com/reaction/1766685

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethyl OxalateHCID 7268—
ReactantHCID 23031084HCID 23031084—
ProductHCID 21110635HCID 2111063593.5%

Reaction Conditions

Temperature120 °C

Reaction Steps

To 4-(7-amino-5-methylindan-4-yloxy)-2-ethyl-3-methylphenol (12 mg) was added diethyl oxalate (150 mg), and the mixture was stirred under an argon atmosphere at 120° C. for 3 hours. The reaction mixture was purified by thin layer chromatography on silica gel (developing solvent: hexane/ethyl acetate=2/1) to give the title compound (15 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07230031B2
Source datasetuspto-grants-2007_06
ORD IDord-bfadfe816abe473fa75eb12b46690e87
Source noteuspto-grants-2007_06