HuagongsheHuagongshe Chemistry Print Report · For research reference only
Anthranilic Acid → 70346-37-1
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Anthranilic Acid | HCID 227 | — |
| Reactant | Ammonia methanol | HCID 21705897 | — |
| Product | 70346-37-1 | HCID 67362646 | 94% |
Reaction Steps
In a 50 mL volume glass vessel equipped with a stirrer and a thermometer were placed 5.0 g (36.5 mmol) of anthranilic acid and 20 mL (156 mmol) of 15 wt. % ammonia methanol solution. The reaction was carried out for 2 hours at room temperature. After the reaction was complete, the reaction mixture was concentrated under reduced pressure, to obtain 5.0 g (isolated yield: 94%) of ammonium anthranilate as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07232903B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-b7c18331578d4359a5aea05328154574 |
| Source note | uspto-grants-2007_06 |