ETHYL 2-AMINO-5-IODOBENZOATE → HCID 69507674, compound

HRID 1767220Notes

Reaction equation

HRID 1767220 reaction equation
[CH2:1]([O:8][C:9]1[CH:14]=[CH:13][C:12]([CH3:15])=[CH:11][C:10]=1[C:16]1[CH2:20][CH2:19][CH2:18][C:17]=1B(O)O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:24]([O:26][C:27](=[O:36])[C:28]1[CH:33]=[C:32](I)[CH:31]=[CH:30][C:29]=1[NH2:35])[CH3:25]>>[CH2:24]([O:26][C:27](=[O:36])[C:28]1[C:29]([NH2:35])=[CH:30][CH:31]=[C:32]([C:17]2[CH2:18][CH2:19][CH2:20][C:16]=2[C:10]2[CH:11]=[C:12]([CH3:15])[CH:13]=[CH:14][C:9]=2[O:8][CH2:1][C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)[CH:33]=1)[CH3:25]

Participants

3

Reactant 2

HCID 12012179ETHYL 2-AMINO-5-IODOBENZOATEHCID 21112913HCID 21112913, compound

Product 1

HCID 69507674HCID 69507674, compound

Procedure

Prepared by general procedure C(iii) but using 2-(2-benzyloxy-5-methylphenyl)cyclopentene-1-boronic acid instead of 2-(2-benzyloxy-5-chlorophenyl)cyclopentene-1-boronic acid and 2-amino-5-iodobenzoic acid ethyl ester instead of 2-chloropyrimidine-4-carboxylic acid methyl ester.

Workup

  1. customPrepared by general procedure C(iii)

Sources & evidence

ORD record
ord-53d915aa387a4f8c9f1e2ed13c23684f
Source dataset
uspto-grants-2007_06
Patent number
US07232821B2

Reaction notes

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