HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 11430183, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86589220 | HCID 86589220 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 11430183 | HCID 11430183 | — |
Reaction Steps
Compound 4 was prepared from {5-dimethylamino-2-[3-oxo-3-(3-pyridin-3-yl-phenyl)-propionylamino]-4-trifluoromethyl-phenyl}-carbamic acid tert-butyl ester (M1) (306 mg, 0.56 mmol) by treatment with TFA in CH2Cl2 according to the general procedure N. Obtained as a yellow solid (162 mg). MS (ISP) 425.4 [(M+H)+]; mp 204° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07235547B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-2144934f802b4a3aa2139fa2513f0149 |
| Source note | uspto-grants-2007_06 |