HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → 2-Acetamidophenylboronic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | (2-Aminophenyl)boronic acid | HCID 2773216 | — |
| Product | 2-Acetamidophenylboronic acid | HCID 2737789 | 63.5% |
Reaction Steps
A mixture of 2-aminophenylboronic acid (900 mg; 6.6 mmol), triethylamine (0.57 ml; 7 mmol) and acetylchloride (0.5 ml; 7 mmol) was stirred at rt. for 1 h. The reaction mixture was evaporated to dryness, stirred with H2O and filtered to give 750 mg (63%) product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07235548B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-2ace11fd48294c6085ef14e537ac708d |
| Source note | uspto-grants-2007_06 |