HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → 2-Methyl-4(3H)-quinazolinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Anthranilamide | HCID 6942 | — |
| Product | 2-Methyl-4(3H)-quinazolinone | HCID 135400457 | — |
Reaction Steps
A solution of anthranilamide (13.6 g; 100 mmol) in acetic acid (100 ml) was refluxed for 60 h. The reaction mixture was evaporated to dryness, suspended in H2O, filtered and washed thoroughly with NaHCO3 until the filtrate had a pH of 8–8.5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07235548B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-6cf122485f9a49e6bbb62cd26fcd4c64 |
| Source note | uspto-grants-2007_06 |