(3-Methoxyphenyl)boronic acid → HCID 22324086, compound

HRID 1767647Notes

Reaction equation

HRID 1767647 reaction equation
[CH:1]1([CH:7]2[NH:12][C:11]3[CH:13]=[CH:14][CH:15]=[C:16](C4C=CC=CC=4OC)[C:10]=3[S:9](=[O:26])(=[O:25])[NH:8]2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[CH3:27][O:28][C:29]1[CH:30]=[C:31](B(O)O)[CH:32]=[CH:33][CH:34]=1>[Pd]>[CH:1]1([CH:7]2[NH:12][C:11]3[CH:13]=[CH:14][CH:15]=[C:16]([C:33]4[CH:32]=[CH:31][CH:30]=[C:29]([O:28][CH3:27])[CH:34]=4)[C:10]=3[S:9](=[O:26])(=[O:25])[NH:8]2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

4

Reactant 2

HCID 2734370(3-Methoxyphenyl)boronic acidHCID 22324109HCID 22324109, compound

Product 1

HCID 22324086HCID 22324086, compound

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

Synthesis as for compound 80 (using 3-methoxyphenylboronic acid for the Pd-cat. cross coupling). M.p. 108–115° C.

Sources & evidence

ORD record
ord-c9420677a821424cb6866043fa0a9282
Source dataset
uspto-grants-2007_06
Patent number
US07235548B2

Reaction notes

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