HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanaminium, N,N,N-tributyl-, fluoride, hydrate → 6-Hydroxyskatole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanaminium, N,N,N-tributyl-, fluoride, hydrate | HCID 16211673 | — |
| Reactant | 1-(tert-butyl-dimethyl-silanyl)-6-(tert-butyl-dimethyl-silanyloxy)-3-methyl-1H-indole | HCID 23614481 | — |
| Product | 6-Hydroxyskatole | HCID 13662595 | — |
Reaction Steps
In analogy to the procedure described in example 3 b], 1-(tert-butyl-dimethyl-silanyl)-6-(tert-butyl-dimethyl-silanyloxy)-3-methyl-1H-indole was treated with tetrabutylammonium fluoride hydrate to obtain 3-methyl-1H-indol-6-ol as brown crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07235572B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-2bc6182bf1af4488870d921d77ef4e37 |
| Source note | uspto-grants-2007_06 |