HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2-Chlorotrityl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | (2-Chlorophenyl)diphenylmethanol | HCID 298659 | — |
| Product | 2-Chlorotrityl chloride | HCID 94524 | 82% |
Reaction Steps
Following the procedure outlined in Example 4, 5.00 g (17.1 mmol) of (2-chlorophenyl) diphenyl methanol, designated as T-3 on Appendix A, was treated with 2.5 ml thionyl chloride (34 mmol) according to general method B to give 4.39 g (82%) of (2-Chlorophenyl) diphenyl chloromethane, mp: 131° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07235577B1 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-ea878467a0cc43d78cb61fe7ac86d6ed |
| Source note | uspto-grants-2007_06 |