HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxyphenol → HCID 9836196, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxyphenol | HCID 9007 | — |
| Reactant | 3-(3-Methoxyphenyl)-2-cyano-acrylic acid ethyl ester | HCID 367497 | — |
| Product | HCID 9836196 | HCID 9836196 | 0.2% |
Reaction Steps
The title compound was prepared from 3-methoxyphenol and 3-(3-methoxyphenyl)-2-cyano-acrylic acid ethyl ester by a procedure similar to that described for Example 16 in 0.2% yield. 1H NMR (CDCl3): 7.50 (t, J=8.1 Hz, 1H), 7.32 (d, J=8.7 Hz, 1H), 7.12 (dd, J=8.4, 2.4 Hz, 1H), 7.03-6.96 (m, 2H), 6.90-6.83 (m, 2H), 3.93 (s, 3H), 3.87 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07235674B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-8716594e50ce4287b3a393a6f253f3d9 |
| Source note | uspto-grants-2007_06 |