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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1768609Generated: November 3, 2026

Salicylaldehyde → 2-(2-Hydroxyethoxy)benzaldehyde

https://huagongshe.com/reaction/1768609

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSalicylaldehydeHCID 6998—
ReactantEthylene carbonateHCID 7303—
CatalystTetraethylammonium BromideHCID 6285—
SolventEthyl AcetateHCID 8857—
Product2-(2-Hydroxyethoxy)benzaldehydeHCID 93989—

Reaction Conditions

Temperature140 °C

Reaction Steps

A mixture of 0.2 mol of 2-hydroxybenzaldehyde, 0.2 mol of ethylene carbonate and 0.3 mol of tetraethylammonium bromide was heated at 140° C. for 2 hours. After cooling, the reaction mixture was taken up in ethyl acetate, washed with water, dried over MgSO4 and evaporated. The compound was purified by distillation.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05378718
Source datasetuspto-grants-1995_01
ORD IDord-dff2944299ed43279ff4f0401f82f5ad
Source noteuspto-grants-1995_01