HuagongsheHuagongshe Chemistry Print Report · For research reference only
Salicylaldehyde → 2-(2-Hydroxyethoxy)benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Salicylaldehyde | HCID 6998 | — |
| Reactant | Ethylene carbonate | HCID 7303 | — |
| Catalyst | Tetraethylammonium Bromide | HCID 6285 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 2-(2-Hydroxyethoxy)benzaldehyde | HCID 93989 | — |
Reaction Conditions
| Temperature | 140 °C |
|---|
Reaction Steps
A mixture of 0.2 mol of 2-hydroxybenzaldehyde, 0.2 mol of ethylene carbonate and 0.3 mol of tetraethylammonium bromide was heated at 140° C. for 2 hours. After cooling, the reaction mixture was taken up in ethyl acetate, washed with water, dried over MgSO4 and evaporated. The compound was purified by distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05378718 |
| Source dataset | uspto-grants-1995_01 |
| ORD ID | ord-dff2944299ed43279ff4f0401f82f5ad |
| Source note | uspto-grants-1995_01 |