2-Butenoic acid, 3-amino-, ethyl ester, (2Z)- → HCID 18948984, compound

HRID 1768612Notes

Reaction equation

HRID 1768612 reaction equation
[O:1]([CH2:5][CH2:6][O:7][C:8]1[CH:15]=[CH:14][C:11]([CH:12]=O)=[CH:10][CH:9]=1)[N+:2]([O-:4])=[O:3].[NH2:16]/[C:17](/[CH3:24])=[CH:18]\[C:19]([O:21][CH2:22][CH3:23])=[O:20]>C(O)C>[CH2:22]([O:21][C:19]([C:18]1[CH:12]([C:11]2[CH:14]=[CH:15][C:8]([O:7][CH2:6][CH2:5][O:1][N+:2]([O-:4])=[O:3])=[CH:9][CH:10]=2)[C:18]([C:19]([O:21][CH2:22][CH3:23])=[O:20])=[C:17]([CH3:24])[NH:16][C:17]=1[CH3:24])=[O:20])[CH3:23]

Participants

4

Reactant 2

HCID 6437562-Butenoic acid, 3-amino-, ethyl ester, (2Z)-HCID 20095559HCID 20095559, compound

Product 1

HCID 18948984HCID 18948984, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A solution of 5 g of 4-(2-nitroxyethoxy)benzaldehyde and 6.1 g of ethyl 3-aminocrotonate in 100 ml of ethanol was refluxed for 20 hours.

Sources & evidence

ORD record
ord-ce9a69348c254cd4a996a08c417a254d
Source dataset
uspto-grants-1995_01
Patent number
US05378718

Reaction notes

Loading…