HuagongsheHuagongshe Chemistry Print Report · For research reference only
Salicylaldehyde → HCID 20095524, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Salicylaldehyde | HCID 6998 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-Bromo-2,2-dimethyl-1-propanol | HCID 142501 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 20095524 | HCID 20095524 | — |
Reaction Steps
A solution of 20 g of salicylaldehyde, 30 g of 3-bromo-2,2-dimethylpropanol and 22 g of potassium carbonate in DMF was refluxed for 24 hours. After evaporation, the residue was dissolved in ethyl acetate and the solution was washed with water. The organic phase was dried over magnesium sulfate and evaporated. The residue was purified by chromatography (silica; dichloromethane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05378718 |
| Source dataset | uspto-grants-1995_01 |
| ORD ID | ord-55d88e117d97414596a7f0a1bd1d02b9 |
| Source note | uspto-grants-1995_01 |