HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxylamine → HCID 14860703, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxylamine | HCID 787 | — |
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 14212862 | HCID 14212862 | — |
| Product | HCID 14860703 | HCID 14860703 | — |
Reaction Steps
Using 2-acetamido-N-benzyl-2-ethoxyacetamide (2.00 g, 8.0 mmol), BBr3 (1M in CH2Cl2, 8.8 mL, 8.8 mmol), and anhydrous NH2OH (5-6 equiv) gave an oily residue. The residue was separated in three components by flash chromatography on SiO2 gel (7.5% MeOH/CHCl3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05378729 |
| Source dataset | uspto-grants-1995_01 |
| ORD ID | ord-d91efea80aa04d05ad67bcd6c0fcc0e0 |
| Source note | uspto-grants-1995_01 |