Diisopropyl Ether → HCID 10686342, compound

Participants

Reaction Steps

To a solution of 24.03 g of Compound 2 obtained in the above step (2) in 40 ml of methylene chloride is added 21.2 g of 80% m-chloroperbenzoic acid at room temperature, and the resultant mixture is stirred for 45 minutes. The reaction mixture is mixed with isopropyl ether and the crystals are filtered to give 25.06 g of the titled compound 1as crystals. Yield: 99%

Provenance & Evidence