HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexylamine → HCID 20098397, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | HCID 15611138 | HCID 15611138 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20098397 | HCID 20098397 | — |
Reaction Steps
2.5 g of 2-[(2-oxiranyl)methoxy]-N-(1H-indol-4-yl)-benzamide in 20 ml of ethanol was refluxed for 2 hours with 1.86 ml of cyclohexylamine and the solvent was eliminated under reduced pressure. The residue was chromatographed over silica (eluent:chloroform-methanol 9-1) to obtain 1.97 g of 2-[3-(cyclohexylamino)-2-hydroxypropoxy]-N-(1H-indol-4-yl)-benzamide
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05380722 |
| Source dataset | uspto-grants-1995_01 |
| ORD ID | ord-8a54c689504442a1b1cc2dd8ebb438df |
| Source note | uspto-grants-1995_01 |