Iodoethane → HCID 18947046, compound

Participants

Reaction Steps

3.75 ml of a 1.6M solution of n-butyllithium in hexane are added, at -70° C., to a solution of 1.4 g of 5-tosyl-5,6-dihydro-4H-thieno[3,4-c]pyrrole in 15 ml of dry tetrahydrofuran. 0.51 ml of iodoethane is then added and the mixture is stirred at room temperature for 2 h and the solution is then poured into 100 ml of ice-cold water. The solid formed is filtered off, washed with hexane and recrystallized from ethanol. 0.16 g of product is obtained. Melting point: 117°-120° C.

Provenance & Evidence