3-Mercaptopropionic Acid → HCID 21884966, compound

HRID 1769398Notes

Reaction equation

HRID 1769398 reaction equation
[SH:1][CH2:2][CH2:3][C:4]([OH:6])=[O:5].[CH2:7]([Sn:11](=O)[CH2:12][CH2:13][CH2:14][CH3:15])[CH2:8][CH2:9][CH3:10]>>[SH:1][CH2:2][CH2:3][C:4]([O-:6])=[O:5].[CH2:7]([Sn+2:11][CH2:12][CH2:13][CH2:14][CH3:15])[CH2:8][CH2:9][CH3:10].[SH:1][CH2:2][CH2:3][C:4]([O-:6])=[O:5]

Participants

3

Reactant 2

HCID 65143-Mercaptopropionic AcidHCID 61221Dibutyltin oxide

Product 1

HCID 21884966HCID 21884966, compound

Procedure

A mixture of 2.475 kg (23.3 tool) of 3-mercaptopropionic acid and 5.97 kg (24 mol) of dibutyltin oxide is continuously fed into a screw drier whose heat exchange areas consist of two heating and one cooling zone. Behind each heating zone, a suction device is present for removing the water of reaction formed.

Workup

  1. temperatureheat exchange areas
  2. customfor removing
  3. customthe water of reaction
  4. customformed

Sources & evidence

ORD record
ord-8025896bdfce48adaac19ed58a87487b
Source dataset
uspto-grants-1995_01
Patent number
US05380896

Reaction notes

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