HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Ethylenedioxy-4-(3,4',5'-trifluorophenyl)-3-cyclohexen → 1,1-Ethylenedioxy4-(3',4',5'-trifluorophenyl)-cyclohexane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Ethylenedioxy-4-(3,4',5'-trifluorophenyl)-3-cyclohexen | HCID 57214902 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1,1-Ethylenedioxy4-(3',4',5'-trifluorophenyl)-cyclohexane | HCID 86748400 | 94.3% |
Reaction Steps
1,1-Ethylenedioxy-4-(3,4',5'-trifluorophenyl)-3-cyclohexen (100 g) was dissolved in ethanol (1 l), followed by adding Pd/C (5%) (40 g), stirring the mixture in a hydrogen gas atmosphere to carry out a catalytic reduction, filtering off the catalyst after the reaction, and distilling off the organic layer under reduced pressure, to obtain 1,1-ethylenedioxy4-(3',4',5'-trifluorophenyl)-cyclohexane (95 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05382379 |
| Source dataset | uspto-grants-1995_01 |
| ORD ID | ord-26e54719b127415fb91831dd7ea06e5c |
| Source note | uspto-grants-1995_01 |