6-Amino-1-hexanol → HCID 178459129, compound

HRID 1769588Notes

Reaction equation

HRID 1769588 reaction equation
[CH3:1][CH:2]([CH3:4])[O-:3].[CH3:5][CH:6]([CH3:8])[O-:7].[CH3:9][CH:10]([CH3:12])[O-:11].[Ti+3:13].[NH2:14]CCCCCCO>>[CH3:1][CH:2]([CH3:4])[O-:3].[CH3:5][CH:6]([CH3:8])[O-:7].[CH3:9][CH:10]([CH3:12])[O-:11].[NH2:14][Ti+3:13][CH2:1][CH2:2][CH2:4][CH2:5][CH2:6][CH3:8]

Participants

3

Reactant 2

HCID 199606-Amino-1-hexanolHCID 9815954titanium(3+) propan-2-olate

Product 1

HCID 178459129HCID 178459129, compoundYield 200%

Procedure

0.1 moles of titanium-tri-isopropoxide (Tyzor TPT Dupont, Wilmington, Del.) and 0.1 moles of 6-amino-1-hexanol were added to a 50 ml beaker and stirred at room temperature for 1 minute to form 0.1 mole of amino-hexyl-titanium-tri-isopropoxide. The reaction mixture was heated to 70° C. for 10 minutes to evaporate the isopropyl alcohol formed during the reaction.

Sources & evidence

ORD record
ord-67ab2309cf784c37b94831901886f134
Source dataset
uspto-grants-1995_01
Patent number
US05382468

Reaction notes

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