1,6-Hexanediol → HCID 178459130, compound

HRID 1769589Notes

Reaction equation

HRID 1769589 reaction equation
[CH3:1][CH:2]([CH3:4])[O-:3].[CH3:5][CH:6]([CH3:8])[O-:7].[CH3:9][CH:10]([CH3:12])[O-:11].[Ti+3:13].O[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20]O>>[CH3:1][CH:2]([CH3:4])[O-:3].[CH3:5][CH:6]([CH3:8])[O-:7].[CH3:9][CH:10]([CH3:12])[O-:11].[OH:3][Ti+3:13][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20]

Participants

3

Reactant 2

HCID 123741,6-HexanediolHCID 9815954titanium(3+) propan-2-olate

Product 1

HCID 178459130HCID 178459130, compoundYield 200%

Procedure

0.1 moles of titanium-tri-isopropoxide (Tyzor TPT DuPont, Wilmington, Del.) and 0.1 moles of 6-hydroxy-1-hexanol were added to a 50 ml beaker and stirred at room temperature for 1 minute to form 0.1 mole of hydroxy-hexyl-titanium-tri-isopropoxide. The reaction mixture was heated to 70 degrees C. for 10 minutes to evaporate the isopropyl alcohol formed during the reaction.

Sources & evidence

ORD record
ord-8657c1b3de264d7cb0ce78307f9af60d
Source dataset
uspto-grants-1995_01
Patent number
US05382468

Reaction notes

Loading…