HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromohexane → HCID 54725955, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromohexane | HCID 8101 | — |
| Reactant | 5-methyl-2,4-dihydro-1H-3,1-benzoxazine-2,4-dione | HCID 10487522 | — |
| Reactant | HCID 135795656 | HCID 135795656 | — |
| Product | HCID 54725955 | HCID 54725955 | — |
Reaction Steps
The 1-hexyl-3-formyl-4-hydroxy-6-methyl-2(1H)-quinolinone was obtained by following Steps (2) to (4) of Preparation A wherein hexyl bromide was reacted with 6-methyl-isatoic anhydride to produce 1-hexyl-4-hydroxy-6-methyl-2(1H)-quinolinone. Then the 1-hexyl-4-hydroxy-6-methyl-2(1H)-quinolinone was converted to 1-hexyl-3-formyl-4-hydroxy-6-methyl-2(1H)-quinolinone following the procedure of Preparation B.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05382572 |
| Source dataset | uspto-grants-1995_01 |
| ORD ID | ord-d614703836324a47956620ed692f924d |
| Source note | uspto-grants-1995_01 |