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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1769625Generated: November 2, 2026

Benzeneacetamide, N-methoxy- → HCID 10330393, compound

https://huagongshe.com/reaction/1769625

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzeneacetamide, N-methoxy-HCID 326647—
ReactantTert-Butyl hypochloriteHCID 521297—
SolventChloroformHCID 6212—
ProductHCID 10330393HCID 10330393—

Reaction Conditions

Temperature0 °C

Reaction Steps

Dissolve 1.65 g (10 mmol) of N-(methoxy)-phenylacetamide in 30 cm3 of dry chloroform. Place in an ice-bath and maintain at a temperature of 0° C. Subsequently, pour in progressively, using a flask, 1.30 g (1.36 cm3, 12 mmol) of tert-butyl hypochlorite which has previously been dissolved in 20 cm3 of chloroform.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05382593
Source datasetuspto-grants-1995_01
ORD IDord-34ec70b5e99344f9b8cc44edec933826
Source noteuspto-grants-1995_01