m-Tolyl isocyanate → HCID 14996869, compound

Participants

Reaction Steps

The procedure is analogous to that described in Example 1, but 1.2 g of 2-amino-N-[2-oxo-2-(1perhydroazepinyl)ethyl]-N-phenylacetamide and 0.55 g of 3-methylphenyl isocyanate are used as the starting material. After recrystallization from a mixture of dimethylformamide and ethyl acetate (63-35 by volume), 0.9 g of N-[2-oxo-2-(1-perhydroazepinyl)ethyl]-2-[3-(3-methylphenyl)ureido]-N-phenylacetamide melting at 245° C. is obtained.

Provenance & Evidence