HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → Benzenesulfonic acid, 4-methyl-, compd. with pyridine (1:1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Product | Benzenesulfonic acid, 4-methyl-, compd. with pyridine (1:1) | HCID 466102 | — |
Reaction Steps
The pyridinium p-toluenesulfonate was prepared by swirling 17.1 g (90 mmoles) of p-toluenesulfonic acid monohydrate with 36 ml (450 mmoles) of pyridine at ambient temperature in a 100-ml round-bottomed flask for 20 minutes. Excess pyridine was removed in a rotary evaporator. White crystals formed which were dried in a vacuum oven overnight at 80°. The yield was 21 g (84%), m.p. 120°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05382703 |
| Source dataset | uspto-grants-1995_01 |
| ORD ID | ord-2868c1c341aa48cfa801a46c04174434 |
| Source note | uspto-grants-1995_01 |