Dicyclohexylcarbodiimide → HCID 178447917、化合物

関与物質

反応手順

A mixture of 0.11 mol of DCC add 50 ml of dichloromethane is added at 0° C. to a mixture of 0.1 mol of 3-isopropylidenecyclobutanecarboxylate [sic] (prepared by the method of Gripps et al., Am. Soc. 81 (1959), 2723-2728) 0.1 mol of 4-(trans-4-propylcyclohexyl)phenol and 100 ml of dichloromethane. After the mixture has been stirred at room temperature for 16 hours and the solid constituents have been removed, conventional work-up gives the product.

情報源と証拠