HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1769965Generated: October 26, 2026
Benzyl mercaptan → 2-Benzylthio-3,5-dinitrobenzotrifluoride
https://huagongshe.com/reaction/1769965
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzyl mercaptan | HCID 7509 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Benzene, 2-chloro-1,5-dinitro-3-(trifluoromethyl)- | HCID 67851 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 2-Benzylthio-3,5-dinitrobenzotrifluoride | HCID 13581600 | — |
Reaction Steps
67.6 g of 2-chloro-3,5-dinitrobenzotrifluoride are dissolved in 150 ml of N,N-dimethylformamide (DMF) and the mixture is treated with 35.9 g of solid potassium carbonate, treated dropwise with 31 g of benzylmercaptan in 200 ml of DMF with stirring at 0° C., and subsequently stirred for a further 16 hours at room temperature, while cooling.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05384321 |
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| Source dataset | uspto-grants-1995_01 |
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| ORD ID | ord-110cc9e47bc0458aa870ebcaabb10dfe |
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| Source note | uspto-grants-1995_01 |
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