HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylcarbamoyl Chloride → HCID 10155020, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylcarbamoyl Chloride | HCID 6598 | — |
| Reactant | Tetrafluoro-m-phenylenediamine dihydrochloride | HCID 149026 | — |
| Reactant | HCID 20096592 | HCID 20096592 | — |
| Product | HCID 10155020 | HCID 10155020 | 35.1% |
Reaction Steps
A suspension of 31.2 g (100 mmol) 2-amino-5-(2,4-dichlorobenzylamino)-nitrobenzene is hydrogenated in a manner analogous with Example 1 (variant A) and worked up appropriately with 13.9 g (101 mmol) N,N-dimethylcarbamoyl chloride. 12.4 g of the end product are obtained in the form of the dihydrochloride. This forms colorless to pale pink crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05384330 |
| Source dataset | uspto-grants-1995_01 |
| ORD ID | ord-79e07c8af94c479084e40eeb339278ee |
| Source note | uspto-grants-1995_01 |