Penicillamine → HCID 20095541, compound

HRID 1770204Notes

Reaction equation

HRID 1770204 reaction equation
[CH:1](=O)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].[NH2:8][C@@H:9]([C:14]([OH:16])=[O:15])[C:10]([SH:13])([CH3:12])[CH3:11]>O>[C:14]([CH:9]1[C:10]([CH3:12])([CH3:11])[S:13][CH:1]([CH2:2][CH2:3][CH2:4][CH2:5][CH3:6])[NH:8]1)([OH:16])=[O:15]

Participants

4

Reactant 2

HCID 5852PenicillamineHCID 6184Hexanal

Product 1

HCID 20095541HCID 20095541, compoundYield 60%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

4 g of hexanal were added to a vigorously stirred solution of 9 g of D-penicillamine in 100 ml of H2O. After stirring for 30 minutes, the solid substance was filtered off, washed successively with water and diethyl ether and dried. Yield 60%.

Workup

  1. filtrationthe solid substance was filtered off
  2. washwashed successively with water and diethyl ether
  3. customdried

Sources & evidence

ORD record
ord-b17fbee6d6ee4cb4b0e8e0e82467e940
Source dataset
uspto-grants-1995_01
Patent number
US05385922

Reaction notes

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