HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxybenzaldehyde → Benzaldehyde, 4-(2-hydroxyethoxy)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxybenzaldehyde | HCID 126 | — |
| Reactant | Ethylene carbonate | HCID 7303 | — |
| Catalyst | Tetraethylammonium Bromide | HCID 6285 | — |
| Product | Benzaldehyde, 4-(2-hydroxyethoxy)- | HCID 89178 | 66% |
Reaction Steps
Synthesized from 30 g of 4-hydroxybenzaldehyde, 21 g of ethylene carbonate and 62 g of tetraethylammonium bromide as described in Example XIIa. Purified by distillation (boiling point 0.1 140°-150° C.). Yield 66%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05385922 |
| Source dataset | uspto-grants-1995_01 |
| ORD ID | ord-633732ee002d423cb093001662a2773a |
| Source note | uspto-grants-1995_01 |