HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Hydroxybenzaldehyde → HCID 20095509, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Hydroxybenzaldehyde | HCID 101 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 13807492 | HCID 13807492 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20095509 | HCID 20095509 | 19% |
Reaction Steps
1.42 g of sodium were dissolved in 200 ml of ethanol. 7.5 g of 3-hydroxybenzaldehyde and 10.5 g of bromoethyl nitrate were added and the resulting solution was refluxed for 5 hours. The compound was purified by column chromatography (silica, CH2Cl2). Yield 19%. Melting point: oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05385922 |
| Source dataset | uspto-grants-1995_01 |
| ORD ID | ord-299e2b44d64b4cf7892b706773fbfa08 |
| Source note | uspto-grants-1995_01 |