Chloroacetyl chloride → Chloroacetoxypropyl methacrylate

HRID 1770300Notes

Reaction equation

HRID 1770300 reaction equation
[Cl:1][CH2:2][C:3](Cl)=[O:4].[C:6]([O:11][CH2:12][CH2:13][CH2:14][OH:15])(=[O:10])[C:7]([CH3:9])=[CH2:8]>N1C=CC=CC=1>[C:6]([O:11][CH2:12][CH2:13][CH2:14][O:15][C:3](=[O:4])[CH2:2][Cl:1])(=[O:10])[C:7]([CH3:9])=[CH2:8]

Participants

4

Reactant 2

HCID 6577Chloroacetyl chlorideHCID 176943-Hydroxypropyl methacrylate

Product 1

HCID 23079572Chloroacetoxypropyl methacrylate

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

Chloroacetoxypropyl methacrylate (CAPM) was prepared by condensation of chloroacetyl chloride with hydroxypropyl methacrylate in pyridine (cf Chem. Abs. 68, 105913 g) b.p. 92°-4° C./0.2mm.

Sources & evidence

ORD record
ord-dde79a1c8a1548059752e13f132d737c
Source dataset
uspto-grants-1995_01
Patent number
US05385997

Reaction notes

Loading…