HuagongsheHuagongshe Chemistry Print Report · For research reference only
Styrene → 3,3-Dichloro-1,5-diphenyl-3-silahexane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Styrene | HCID 7501 | — |
| Reactant | 3-Phenyl-1,1-dichloro-1-silabutane | HCID 123324342 | — |
| Catalyst | Chloroplatinic acid | HCID 61859 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | 3,3-Dichloro-1,5-diphenyl-3-silahexane | HCID 21841458 | 74% |
Reaction Steps
In the same apparatus and procedures as EXAMPLE 1, 10.0 g (0.046 mole) of 3-phenyl-1,1-dichloro-1-silabutane, 7.2 g (0.07 mole) of styrene, and 20 μl of 1% chloroplatinic acid in isopropanol were placed and reacted for 3 hours under the dry nitrogen atmosphere at 60° C. Vacuum distillation of the reaction products gave 11.0 g (bp, 133°-5° C./0.6 mmHg) of 3,3-dichloro-1,5-diphenyl-3-silahexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05386050 |
| Source dataset | uspto-grants-1995_01 |
| ORD ID | ord-5c2e2c3b54bd40c493888738b8b2837f |
| Source note | uspto-grants-1995_01 |