Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-(Bromomethyl)-2-fluoro-1-methoxybenzene → 4-(N-(3-fluoro-4-methoxybenzyl)-N-(4-methoxybenzyl)sulfamoyl)-benzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-(Bromomethyl)-2-fluoro-1-methoxybenzene | HCID 2774553 | — |
| 반응물 | Methyl 4-(N-(4-methoxybenzyl)sulfamoyl)benzoate | HCID 26527056 | — |
| 생성물 | 4-(N-(3-fluoro-4-methoxybenzyl)-N-(4-methoxybenzyl)sulfamoyl)-benzoic acid | HCID 57944960 | — |
반응 단계
Prepared as in example 5-10 from 4-(bromomethyl)-2-fluoro-1-methoxybenzene and methyl 4-(N-(4-methoxybenzyl)sulfamoyl)benzoate (example 5-10b). MS (M−H, 458.10); NMR (400 MHz, CD3OD): δ, ppm: 3.73 (s, 3H), 3.80 (s, 3H), 4.24 (s, 2H), 4.28 (s, 2H), 6.75 (m, 4H), 6.88 (m, 1H), 6.97 (d, 2H, J=8.6 Hz), 7.88 (d, 2H, J=8.3 Hz), 8.14 (d, 2H, J=8.3 Hz).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09247759B2 |
| 출처 데이터셋 | uspto-grants-2016_02 |
| ORD ID | ord-67919c3ffcc24082a8309ea933a4d78a |
| 출처 메모 | uspto-grants-2016_02 |