HCID 67508320, compound → HCID 86665516, compound

Participants

Reaction Steps

To a solution of benzyl 4-(2-(2-(2-acetoxyethoxy)ethoxy)ethylsulfonyl)-2-methylbutan-2-ylcarbamate (440.2 mg, 0.959 mmol) in methanol (5 ml) was added Pd on carbon (10%, 83 mg). The suspension was put under a N2 atmosphere and H2 (1.3 atm) introduced. The suspension was stirred for 1.5 hours, filtered (0.45 um, PTFE), and concentrated in vacuo. The residue was used without any further purification. LRMS (ESI/APCI) m/z 326 [M+H]+.

Provenance & Evidence