HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → 10-Carboxydecyl 5-amino-4-oxopentanoate hydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | 10-(benzyloxycarbonyl)decyl 5-(Cbz-amino)-4-oxopentanoate | HCID 90034560 | — |
| Edukt | HCID 178418361 | HCID 178418361 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Isopropanol | HCID 3776 | — |
| Produkt | 10-Carboxydecyl 5-amino-4-oxopentanoate hydrochloride | HCID 90034564 | 51,7% |
Reaktionsschritte
This compound was prepared from the product of 13b (0.60 g; 1.1 mmol), 12 M HCl (0.09 mL; 1.1 mmol), 10% Pd/C (100 mg), hydrogen gas, and 2-propanol (25 mL) using the procedure in Example 8d. 0.20 g (51%) product was obtained (white solid).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09249086B2 |
| Quelldatensatz | uspto-grants-2016_02 |
| ORD ID | ord-4343970d32d849169f01b05cd01c72bc |
| Quellennotiz | uspto-grants-2016_02 |