HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1771118Generated: November 3, 2026
Hydrochloric Acid → Propanoic acid, 3-ethoxy-3-imino-, ethyl ester
https://huagongshe.com/reaction/1771118
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Ethyl cyanoacetate | HCID 7764 | — |
| Product | Propanoic acid, 3-ethoxy-3-imino-, ethyl ester | HCID 75346 | 91.6% |
Reaction Steps
113 g 2-cyanoacetic acid ethyl ester (1 mol) and 1000 mL anhydrous ethyl alcohol were added to a three-necked bottle, into which hydrogen chloride gas was bubbled with stirring at 0° C. After 4 hours, a lot of white solid were isolated and the reaction was stopped. After sucking filtration and drying, 60.0 g white solid was obtained. Yield: 91.6%, MS: 160 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09249106B2 |
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| Source dataset | uspto-grants-2016_02 |
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| ORD ID | ord-de12c632508a46d88f2c6ece429ccaf5 |
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| Source note | uspto-grants-2016_02 |
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